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The Resource Advanced Synthesis of Gold and Zirconia Nanoparticles and their Characterization

Advanced Synthesis of Gold and Zirconia Nanoparticles and their Characterization

Label
Advanced Synthesis of Gold and Zirconia Nanoparticles and their Characterization
Title
Advanced Synthesis of Gold and Zirconia Nanoparticles and their Characterization
Creator
Contributor
Subject
Genre
Language
ger
Summary
The development of small and smallest particle is one of today's key features in modern science. The goal is to form materials with improved properties than their "classical" ancestors with just a fractional amount of raw material. However, the characterization of these particles is as important as their way of preparation. Different techniques with their origins in physics, inorganic, organic and physical chemistry have to be combined to reveal the secrets of this important field of science. This book gives a short overview of theoretical basics and synthesis methods to form and characterize gold and zirconia nanoparticles. Phenomenon like plasmon resonance self-assembly of surfactants and the different structures of ZnO2 are explained. Furthermore, analytical tools, like small angle X-ray scattering, X-ray powder diffraction and scanning electron microscopy are introduced. In addition, details on the synthesis of gold and zirconia nanoparticles are presented and are examined by the mentioned analytical and calorimetric methods. Biographische Informationen Stephan Dankesreiter, Dipl. Chem. (univ.), was born 1984 in Zwiesel. After his basic studies at the University of Regensburg, he joined the COSOM-program (Complex Condensed Materials and Soft Mater) and was able to get a closer look on synthesis and characterization methods of nanoparticles. In 2009, he was able to work on this field during his diploma-thesis at the University of Florence (CSGI, Center for Colloidal and surface science) and finished successfully his studies in chemistry with the diploma degree
Cataloging source
MiAaPQ
LC call number
QD181.A9 -- D36 2011eb
Literary form
non fiction
Nature of contents
dictionaries
Label
Advanced Synthesis of Gold and Zirconia Nanoparticles and their Characterization
Link
http://ebookcentral.proquest.com/lib/multco/detail.action?docID=673417
Instantiates
Publication
Copyright
Carrier category
online resource
Carrier category code
cr
Carrier MARC source
rdacarrier
Color
multicolored
Content category
text
Content type code
txt
Content type MARC source
rdacontent
Contents
  • Advanced Synthesis of Gold and Zirconia Nanoparticles and their Characterization -- Table of Contents -- Part I. Introduction -- Part II. Fundamentals -- 1. Plasma oscillation and Mie's theory -- 1.1 Principles of plasma oscillation -- 1.2 Scattering and absorption of small particles -- 2. L(+)-ascorbic acid and its derivates -- 2.1 Chemical properties of ascorbic acid -- 2.2 AscX surfactants and their aggregates -- 2.3 The formation of gel and coagel -- 3. Zirconia and its different structures and species -- 3.1 Zirconyl chloride in aqueous solutions -- 3.2 Structures of zirconium oxide -- 4. Structural investigation techniques -- 4.1 X-ray based methods -- 4.2 Electron based method: scanning electron microscopy (SEM) -- Part III. Experimental -- 5. Chemicals -- 5.1 Preparation of Gold Nanoparticles -- 5.2 Preparation of zirconium-based nanoparticles -- 6. Analytical Methods -- 6.1 Thermogravimetric analysis (TGA) -- 6.2 Differential scanning calorimetry (DSC) -- 6.3 Bright field and phase contrast microscopy -- 6.4 UV/Vis absorption -- 6.5 Raman measurements -- 6.6 Small angle X-ray scattering (SAXS) -- 6.7 X-ray diffraction (XRD) -- 6.8 Scanning electron microscopy (SEM) -- 7. Synthesis of L(+)ascorbyl stearate (Asc18) -- 8. Synthesis of Gold Nanoparticles -- 8.1 Preparation with Asc18 surfactant -- 8.2 Preparation with Asc12 surfactant -- 8.3 Preparation with Asc14 Asc10 and Asc8 surfactants -- 9. Preparation of ZrO2- nanoparticles -- 9.1 Synthesis of zirconium hydroxide by coprecipitation in homogeneous phase (sol) -- 9.2 Preparation of hydrous zirconia gel -- Part IV. Results and Discussion -- 10. Gold nanoparticles -- 10.1 Determination of the cmt of Asc18 -- 10.2 Synthesized nanoparticles and their colors -- 10.3 UV-Vis characterization -- 10.4 SAXS characterization -- 10.5 Conclusion -- 11. 3. Zirconium hydroxide and oxide nanoparticles
  • 11.1 Raman characterization -- 11.2 Dialysis of the sol and an aqueous ZrOCl2 solution -- 11.3 Characterization with microscopic methods -- 11.4 DSC measurements of the gel -- 11.5 Characterization by SEM -- 11.6 SAXS characterization of the gel -- 11.7 TGA and DTG measurements -- 11.8 XRD characterization of calcined samples -- 11.9 Conclusion -- Part V. Annex
Control code
EBC673417
Dimensions
unknown
Edition
1st ed.
Extent
1 online resource (169 pages)
Form of item
online
Isbn
9783836641999
Media category
computer
Media MARC source
rdamedia
Media type code
c
Note
Electronic reproduction. Ann Arbor, Michigan : ProQuest Ebook Central, 2017. Available via World Wide Web. Access may be limited to ProQuest Ebook Central affiliated libraries.
Sound
unknown sound
Specific material designation
remote
System control number
  • (MiAaPQ)EBC673417
  • (Au-PeEL)EBL673417
  • (CaPaEBR)ebr10489404
  • (OCoLC)709551434
Label
Advanced Synthesis of Gold and Zirconia Nanoparticles and their Characterization
Link
http://ebookcentral.proquest.com/lib/multco/detail.action?docID=673417
Publication
Copyright
Carrier category
online resource
Carrier category code
cr
Carrier MARC source
rdacarrier
Color
multicolored
Content category
text
Content type code
txt
Content type MARC source
rdacontent
Contents
  • Advanced Synthesis of Gold and Zirconia Nanoparticles and their Characterization -- Table of Contents -- Part I. Introduction -- Part II. Fundamentals -- 1. Plasma oscillation and Mie's theory -- 1.1 Principles of plasma oscillation -- 1.2 Scattering and absorption of small particles -- 2. L(+)-ascorbic acid and its derivates -- 2.1 Chemical properties of ascorbic acid -- 2.2 AscX surfactants and their aggregates -- 2.3 The formation of gel and coagel -- 3. Zirconia and its different structures and species -- 3.1 Zirconyl chloride in aqueous solutions -- 3.2 Structures of zirconium oxide -- 4. Structural investigation techniques -- 4.1 X-ray based methods -- 4.2 Electron based method: scanning electron microscopy (SEM) -- Part III. Experimental -- 5. Chemicals -- 5.1 Preparation of Gold Nanoparticles -- 5.2 Preparation of zirconium-based nanoparticles -- 6. Analytical Methods -- 6.1 Thermogravimetric analysis (TGA) -- 6.2 Differential scanning calorimetry (DSC) -- 6.3 Bright field and phase contrast microscopy -- 6.4 UV/Vis absorption -- 6.5 Raman measurements -- 6.6 Small angle X-ray scattering (SAXS) -- 6.7 X-ray diffraction (XRD) -- 6.8 Scanning electron microscopy (SEM) -- 7. Synthesis of L(+)ascorbyl stearate (Asc18) -- 8. Synthesis of Gold Nanoparticles -- 8.1 Preparation with Asc18 surfactant -- 8.2 Preparation with Asc12 surfactant -- 8.3 Preparation with Asc14 Asc10 and Asc8 surfactants -- 9. Preparation of ZrO2- nanoparticles -- 9.1 Synthesis of zirconium hydroxide by coprecipitation in homogeneous phase (sol) -- 9.2 Preparation of hydrous zirconia gel -- Part IV. Results and Discussion -- 10. Gold nanoparticles -- 10.1 Determination of the cmt of Asc18 -- 10.2 Synthesized nanoparticles and their colors -- 10.3 UV-Vis characterization -- 10.4 SAXS characterization -- 10.5 Conclusion -- 11. 3. Zirconium hydroxide and oxide nanoparticles
  • 11.1 Raman characterization -- 11.2 Dialysis of the sol and an aqueous ZrOCl2 solution -- 11.3 Characterization with microscopic methods -- 11.4 DSC measurements of the gel -- 11.5 Characterization by SEM -- 11.6 SAXS characterization of the gel -- 11.7 TGA and DTG measurements -- 11.8 XRD characterization of calcined samples -- 11.9 Conclusion -- Part V. Annex
Control code
EBC673417
Dimensions
unknown
Edition
1st ed.
Extent
1 online resource (169 pages)
Form of item
online
Isbn
9783836641999
Media category
computer
Media MARC source
rdamedia
Media type code
c
Note
Electronic reproduction. Ann Arbor, Michigan : ProQuest Ebook Central, 2017. Available via World Wide Web. Access may be limited to ProQuest Ebook Central affiliated libraries.
Sound
unknown sound
Specific material designation
remote
System control number
  • (MiAaPQ)EBC673417
  • (Au-PeEL)EBL673417
  • (CaPaEBR)ebr10489404
  • (OCoLC)709551434

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